Sol-gel synthesis of fluorescent materials based on barium aluminate

Barium aluminate was obtained by sol-gel method. We used a heat treatment in an oven at 130°C, and microwave radiation for drying the gel. To obtain a crystalline product all samples were calcined in the muffle furnace at the temperatures up to 1100°C. Complex studies were used...

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Bibliographic Details
Published in:AIP Conference Proceedings Vol. 1772. P. 020008-1-020008-8
Other Authors: Selyunina, Liliya A., Kuznetsova, Ekaterina E, Belyaninova, Tatyana V, Mishenina, Lyudmila N.
Format: Article
Language:English
Subjects:
Online Access:http://vital.lib.tsu.ru/vital/access/manager/Repository/vtls:000563102
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024 7 |a 10.1063/1.4964530  |2 doi 
035 |a to000563102 
039 9 |a 201702140958  |c 201702131821  |d VLOAD  |y 201702131525  |z Александр Эльверович Гилязов 
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245 1 0 |a Sol-gel synthesis of fluorescent materials based on barium aluminate  |c L. Selyunina, L. Mishenina, E. Kuznetsova, T. Belyaninova 
504 |a Библиогр.: 12 назв. 
520 3 |a Barium aluminate was obtained by sol-gel method. We used a heat treatment in an oven at 130°C, and microwave radiation for drying the gel. To obtain a crystalline product all samples were calcined in the muffle furnace at the temperatures up to 1100°C. Complex studies were used to identify the dynamics of phase and structural transformations in the synthesis of barium aluminate. The main stages of formation BaAl2O4 were determined by thermal analysis; evolution of phase composition and crystal structure were studied using X-ray diffraction and IR-spectroscopy. The morphology of surface of the barium aluminate was investigated by scanning electron microscope. In the work fluorescent material with composition Ba1-xEuxAl2O4 was obtained. The maximum of luminescent intensity is achieved with content of Eu3+ equal 0.75 mol in the case of processing of gel by microwaves. The phosphor obtained by heat treatment in an oven gel has a composition Ba0.9Eu0.1Al2O4. 
653 |a золь-гель синтез 
653 |a алюминат бария 
653 |a термический анализ 
653 |a флуоресцентные материалы 
653 |a люминофоры 
655 4 |a статьи в журналах  |9 879358 
700 1 |a Selyunina, Liliya A.  |9 160428 
700 1 |a Kuznetsova, Ekaterina E  |9 102345 
700 1 |a Belyaninova, Tatyana V  |9 160429 
700 1 |a Mishenina, Lyudmila N.  |9 101446 
773 0 |t AIP Conference Proceedings  |d 2016  |g Vol. 1772. P. 020008-1-020008-8  |x 0094-243X 
852 4 |a RU-ToGU 
856 7 |u http://vital.lib.tsu.ru/vital/access/manager/Repository/vtls:000563102 
856 |y Перейти в каталог НБ ТГУ  |u https://koha.lib.tsu.ru/cgi-bin/koha/opac-detail.pl?biblionumber=62691 
908 |a статья 
999 |c 62691  |d 62691