Hydride-dehydride fine zirconium powders for pyrotechnics

In this paper, the possibility of obtaining fine zirconium powders by the hydrogenationdehydrogenation method is studied. The main parameters of the technological process that allow obtaining fine zirconium powders for pyrotechnics are determined. Hydrogenation and dehydrogenation of the samples are...

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Bibliographic Details
Published in:International journal of energetic materials and chemical propulsion Vol. 20, № 1. P. 31-43
Other Authors: Amelichkin, Ivan V., Knyazeva, Elena M., Medvedev, Rodion Olegovych, Muslimova, Alexandra V., Nefedov, Roman Andreevich, Orlov, Vladislav Viktorovich, Sachkov, Victor Ivanovich, Sachkova, Anna Sergeevna, Stepanova, Oyuna B., Zhukov, Ilya A.
Format: Article
Language:English
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Online Access:http://vital.lib.tsu.ru/vital/access/manager/Repository/koha:000925383
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245 1 0 |a Hydride-dehydride fine zirconium powders for pyrotechnics  |c I. V. Amelichkin, E. M. Knyazeva, R. O. Medvedev [et al.] 
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504 |a Библиогр.: с. 42-43 
520 3 |a In this paper, the possibility of obtaining fine zirconium powders by the hydrogenationdehydrogenation method is studied. The main parameters of the technological process that allow obtaining fine zirconium powders for pyrotechnics are determined. Hydrogenation and dehydrogenation of the samples are carried out in a rotating quartz tube placed in a furnace at temperatures of 380◦C and 850◦C, respectively. Zirconium hydride is milled using tungsten carbide balls to eliminate the presence of impurities. Thus it is possible to obtain a fine zirconium powder with a number-average particle size of 4.527 +- 2.650 Um and a specific surface area of 0.231 m2/g from the initial electrolytic zirconium powder with a number-average particle size of 220 Um and a specific surface area < 0.1 m2/g. The allowed relative error of measuring the specific surface area is +- 5%. Hence it is possible to reduce the particle size of zirconium powder by 54.6 times without changing the composition. 
653 |a цирконий 
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653 |a дегидрирование 
653 |a гидрирование 
653 |a мелкодисперсные порошки 
655 4 |a статьи в журналах  |9 879358 
700 1 |a Amelichkin, Ivan V.  |9 854595 
700 1 |a Knyazeva, Elena M.  |9 424387 
700 1 |a Medvedev, Rodion Olegovych  |9 489638 
700 1 |a Muslimova, Alexandra V.  |9 854597 
700 1 |a Nefedov, Roman Andreevich  |9 423009 
700 1 |a Orlov, Vladislav Viktorovich  |9 489637 
700 1 |a Sachkov, Victor Ivanovich  |9 387059 
700 1 |a Sachkova, Anna Sergeevna  |9 459779 
700 1 |a Stepanova, Oyuna B.  |9 854598 
700 1 |a Zhukov, Ilya A.  |9 101411 
773 0 |t International journal of energetic materials and chemical propulsion  |d 2021  |g Vol. 20, № 1. P. 31-43  |x 2150-766X 
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