Isolation, identification, and chromatographic separation of N-methyl derivatives of glycoluril

Isolation, identification, and chromatographic separation of N-methyl derivatives of glycoluril

Mono-, di-, and tetramethylglycolurils were synthesized, isolated, and purified. For the first time, the cis- and the trans-isomers of N,N-dimethylglycoluril were isolated as individual substances by semi-preparative HPLC method. The structures of the synthesized compounds were confirmed by 1H NMR,...

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Bibliographic Details
Published in:Chromatographia Vol. 81, № 10. P. 1431-1437
Other Authors: Kotelnikov, Oleg A., Novikov, D. V., Kusherbaeva, V., Gorbin, Sergey I., Tomilova, Evgeniya V., Zhaksynbaeva, A., Dementeva, Natalya B., Malkov, Victor S., Bakibaev, Abdigali A., Kurgachev, Dmitryi A.
Format: Article
Language:English
Subjects:
колоночная жидкостная хроматография
масс-спектрометрия
спектроскопия ядерного магнитного резонанса
метилгликольурил
мебикар
статьи в журналах
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